WebAug 1, 2010 · Diethyl ether was filtered through a column of activated alumina under an atmosphere of argon. Microwave reactions were performed on a Biotage microwave reactor. 1 H and 13 C NMR spectra were recorded on a Bruker DRX-400, a Bruker DRX-500 or a Bruker DRX-600 spectrometer at ambient temperature (300 K), unless otherwise … WebJan 1, 2013 · Wash solvents: NMP, dichloromethane (DCM), N, N -dimethylformamide (DMF), methanol (MeOH), 1 % acetic acid (HOAc) in MeOH. 4. Coupling reagent and chemicals: HBTU, HOBt, DIEA, DIC, NaBH 3 CN, propargylamine, and 5- (2-formyl-3,5-dimethoxyphenoxy)pentanoic acid (o-PALaldehyde, Peptides International). 5.
Success with Microwave Synthesis - Biotage
WebNov 1, 2013 · All reagents and solvents were purchased from commercials sources and were used without further purification. Microwave irradiation was performed in a Biotage Initiator® Microwave with 2-5 mL Biotage reaction vials. Flash column chromatography was performed using prepacked silica cartridges with a flash purification system. WebMicrowave reactor Biotage Initiator 2.0 is located in 48 Fleming. It is an instrument which allows It is an instrument which allows rapid screening and optimization of … how do i find my imr
Microwave Reactor (Biotage) Materials Research …
WebOne of the most valuable aspects of solid-phase extraction is solvent usage reduction. Compared to liquid-liquid extractions, the solvent use is significantly less for solid-phase extractions. ... but the extraction method uses microwave extraction instead. ... Deanna is an Application Chemist at Biotage. She became a part of Biotage in October ... WebJun 4, 2024 · Microwave assisted synthesis using solvents Microwave assisted synthesis without solvents or solvent free conditions The reports on Microwave assisted synthesis are well documented in the literature since last 5 decades, which includes mainly following reactions Figure 2. Figure 2. Various types of Microwave assisted synthesis. Web9 hours ago · Analytical LCMS was performed on a Shimadzu LCMS 2024 using 0.05% formic acid in water as solvent A and 0.05% formic acid ... % B; 0.2 min, 5% B. Biotage Initiator microwave was used for Cu ... how do i find my incorporation date